Chlorhexidine digluconate 20%
SPECIFICATION
Product name: | Chlorhexidine gluconate (digluconate) 20% solution | ||
Nr | Item | Limits | Reference |
1 | Appearance | Almost colorless or pale yellow clear liquid | USP/EP/BP |
2 | Solubility | Miscible with glacial acetic acid and water, miscible three times by its volume with acetone, and five times with dehydrated alcohol, further addition of alcohol or acetone yields a white precipitation | USP |
Miscible with water, with no more than 3 parts of acetoin, and with no more than 5 parts of ethanol (96%) | EP/BP | ||
3 | Identification tests | ||
A (IR) | The IR spectrum from the sample should correspond to reference standard | USP/EP/BP | |
B (TLC) | The principal spot obtained from the test solution in similar color, size and Rf value to that obtained from the reference standard solution | USP/EP/BP | |
C (Melting point) | Between 132 °C and 136 °C | USP/EP/BP | |
D (Analytical test) | A deep red colour should be produced | USP/EP/BP | |
4 | Specific gravity | Between 1.06 and 1.07 | USP/EP/BP |
5 | pH(5% v/v) | Between 5.5 and 7.0 | USP/EP/BP |
6 | Related substance | NMT 3.0% | USP/EP/BP |
7 | p-Chloraniline | Less than 500 ppm | USP |
Less than 50 pp, | In-house statndard | ||
Complies test | EP/BP | ||
8 | Assay | NLT 19.0% and NMT 21% of chlorhexidine bigluconate | USP |
NLT 190 g/L and NMT 210 g/L of chlorhexidine bigluconate | EP/BP |